9 Characterizing Material Properties

Characterizing Material Properties

This lab is designed to align with AAOT science outcome #1: Gather, comprehend, and communicate scientific and technical information in order to explore ideas, models, and solutions and generate further questions.

Materials

  • writing utensil
  • calculator
  • digital device with spreadsheet program
  • digital device with internet access

ObjectiveS

  1. Identify regions and features of the stress vs. strain curve.
  2. Analyze the features of the stress vs. strain curve to assess qualitative material properties.
  3. Analyze stress vs. strain data to determine ultimate strength and elastic modulus.
  4. Analyze stress vs. strain data to determine the elastic potential energy storage capacity of a material.
  5. Compare and contrast stress vs. strain curves and material properties in the context of real-world applications.

QUalitative Characterization of Stress vs. strain behavior

Materials can be categorized as brittle or ductile based on the relative size of their linear and failure regions. A brittle material will fracture or rupture very shortly after reaching the yield point, the point at which the material begins to permanently deform. A ductile material will have a relatively long failure region, corresponding to permanent deformation without fracture or rupture.

image
The straight dashed lines mark the elastic region of the stress vs strain curve. In each case the X marks where the material fractures. Material A has the highest elastic modulus and highest ultimate strength and fractures after little plastic (permanent) deformation. Material B has a slightly smaller elastic modulus, is very brittle because it fractures without any significant plastic deformation. Material C has the lowest elastic modulus and is also relatively ductile. The three deformation diagrams on the right show A and C before breaking and B after breaking. Image Credit: Figure 12.3 by  Steven Earle, Stress and Strain, Physical Geology (Creative Commons Attribution 4.0 International License)

 

Some materials  stretch easily up to a certain point, but then become very stiff and difficult to stretch. This behavior  causes a toe region in their stress vs. strain curves. For example, the stress vs. strain curves of tendons exhibit a toe region do to crimping behavior.

 

Illustrative diagram of showing the (un)crimping of fibers and the corresponding regions of the stress vs. strain curve. There are three distinct regions of the stress/strain curve: (1) the toe region, (2) the linear region, and (3) the yield and failure region. The toe region represents “un-crimping” of the collagen fibrils; toe region ends at about 2% of strain when all crimpled fibers straighten. It is followed by linear region, in which the collagen fibers respond linearly to load. If strain is less than 4%, the tendon will return to its original length when unloaded. Between 4 to 8 per cent of strain the collagen fibers begin to slide past one another as the cross-links start to fail which results in microscopic failure. If strain is more than 8%, macroscopic failure results.  Image Credit: Kelc Robi, Naranda Jakob, Kuhta Matevz and Vogrin Matjaz (May 15th 2013). The Physiology of Sports Injuries and Repair Processes, Current Issues in Sports and Exercise Medicine, Michael Hamlin, Nick Draper and Yaso Kathiravel, IntechOpen, DOI: 10.5772/54234. Creative Commons 3.0 License

 

1) We will measure a stress vs. strain curve for a common hair tie to determine if the material comprising the hair tie exhibits a toe region and categorize the material as brittle or ductile. Based on your experience, do you expect that the hair tie will exhibit a toe region? Explain your reasoning.

 

 

2) Do you expect that the hair tie material will be brittle or ductile? Explain your reasoning.

 

 

Experimental Methods

Data Collection

We will measure a stress-strain curve for a common hair tie using a strength and materials tester as seen in the following video. The data collected in the video is available in an online spreadsheet. You can copy and paste the data into your own spreadsheet for analysis.

Hair tie with the quick links used for attachment to the strength and materials tester.

Data Analysis

Stress and Strain

To calculate stress we will need to know the cross-sectional area of the rubber band. We will assume the band does not thin out as it stretches so we will use the original cross section to calculate the stress throughout the experiment. The result of this approximation is known as the engineering stress. If we were to instead measure and use the changing cross-section throughout the experiment we would be calculating the true stress. The original diameter of the hair tie was measured to be 2.4 mm using calipers (see image below).

Photograph of calipers being used to measure the diameter of the hair tie. Image Credit: Calipers by Lawrence Davis.

3) Calculate the cross-sectional area of the hair tie in units of m2. The hair-tie was looped around the quick-links in the materials tester, so we were actually stretching two strands of the hair tie and you need to double your cross-sectional area value to account for that. Show your work.

 

 

4) Use your spreadsheet and known original length calculate the strain corresponding to each displacement value.

5) Use your spreadsheet and the cross-section you calculate to calculate the stress corresponding to each force value.

6) Plot the stress on the vertical axis and strain on the horizontal axis. Be sure to title your graph and enter axes labels with correct units.

Elastic Modulus (Young’s Modulus)

7) The elastic modulus of the material is defined as the __________ of the graph in the __________ region of the stress vs. strain curve. (Reading your textbook will remind you of how to fill in the blanks).

 

 

8) Create a second plot that only contains the data from the region you answered above. Fit a line to this data and record the fit equation and the R2 here:

 

9) What is the elastic modulus of the hair-tie material?

 

 

10) What is the elastic modulus in units of MPa and also in units of GPa?

 

Ultimate Strength

11) Use your graph or examine your data to find the ultimate strength of the hair tie material. Record the value in units of MPa and also in units of GPa. 

 

 

Conclusions

12) Does the hair tie stress vs. strain curve contain a toe region, and if so, what strain values does it cover? Explain.

 

13) Is the hair tie material brittle or ductile? Explain your reasoning.

 

 

14) Overall, does the hair tie behave according to your original expectations? Explain.

 

 

15) The uncrimping (toe region) of a tendon provides flexibility by allowing the tendon to stretch to occur under small stress and without significant strain to the actual material fibers themselves.  Once the tendon fibers are uncrimped the tendon becomes very stiff to provide stability while the muscles to apply large forces to skeletal system (steep linear region). Tendons are typically relatively brittle, as indicated by rupture soon after failure begins (sharp drop in stress after the yield point). Are hair ties good qualitative models for tendons (do they behave the same)?

 

16) How does the elastic modulus of the hair tie compare to the elastic modulus of a tendon? Provide a ratio of the two values. Also properly cite your source for the tendon value.

 

17) How does the ultimate strength of the hair tie compare to the ultimate strength of a tendon? Provide a ratio of the two values. Also properly cite your source for the tendon value.

 

18) Overall, does the hair tie make a good model for a tendon? Explain.

 

 

Futher Questions

19) Both tendons and the hair tie exhibit a toe region because the fibers of the material must be uncrimped and aligned before actually being stretched. Use the concepts covered in this lab to explain why you think it might be advantageous to have a toe region in the stress vs. strain graph of a hair tie.

 

 

The work done on the hair tie before it breaks is equal to the area under the measured force vs. displacement curve. We can approximate the force vs. displacement area by multiplying each little bit of additional displacement by the average force recorded during that additional displacement and then adding up all of these results. This process, known as numeric integration, essentially breaks the curve into many small rectangles, finds the area of each little rectangle, and adds up all the little areas.

20) Let’s try this with our hair tie. Use your spreadsheet to average the first two force values in the second cell of the new column. Subtract the first displacement from the second in order to find the displacement over which that average force was applied. Continue this pattern for all the force and displacement values until fracture occurred. Make a third column that converts the additional displacement to meters and multiplies by the average force. This will be the work in Joules. The following chart shows an example of what you are trying to create, with made up example values for displacement and force.

Displacement (cm) Force (N) Average Force (N) Additional Displacement (cm) Work (J)
0 0
0.2 1 0.5 0.2 0.001
0.3 2 1.5 .1 .0015
0.5 4 3 0.2 0.0006

 

21) Use your spreadsheet to sum up each little work done to get the total work before rupture. Record here:

22) If you attached a hook to the hair tie and used it to catch a moving object with mass of 0.5kg, how fast could the object be moving without breaking the hair tie? [Hint: To stop the object the hair tie must do an amount of work that is equal to the object’s kinetic energy.]

 

23) From how high would you drop an object in order for it to reach the speed you calculated above?

 

 

In similar fashion, there are limits on how much energy can be transferred to your tendons when pushing off to change direction or landing after a fall.

 

 

 

License

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General Physics Remote Lab Manual Copyright © by Lawrence Davis is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License, except where otherwise noted.

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